How do you calculate acid insoluble ash?
Boil the ash for 5 minutes with 25 mL of hydrochloric acid (~70 g/l) TS; collect the insoluble matter in a sintered crucible, or on an ashless filter-paper, wash with hot water, and ignite at about 500 °C to constant weight.
Calculate the content in mg of acid- insoluble ash per g of air-dried material..
What is water soluble ash value?
Ash value is useful in determining authenticity and purity of sample and also these values are important qualitative standards. The total ash value, acid insoluble ash, water soluble ash was found to be 11.75%, 7.45% and 7.85%. … The Water-soluble extractive value plays an important role in evaluation of crude drugs.
How do you calculate ash value?
Subtract the weight of insoluble matter from the weight of the ash; the difference in weight represents the water- soluble ash. Calculate the percentage of water- soluble ash with reference to the air dried drug.
What is Ash value?
ASH VALUESThe residue remaining after incineration is the ash content of the drug.( inorganic salts of carbonates, phosphates, silicates of sodium, potassium, calcium and magnesium) is known as ash content.Ash value is a criterion to judge the identity OR purity of the crude drug.
Why do we calculate ash value?
Ash values are helpful to determine the quality as well as purity of a crude drug, especially when the drug is present in powdered form. The object of ashing crude drugs is to remove the traces of organic matter which may be interferes in an analytical determination.
Why acid insoluble ash content is important?
I want to know the significance of ash tests performed in physicochemical analysis. Total ash test gives an estimation about purity and quality of drug. Acid insoluble ash value indicates siliceous impurities. Water soluble ash value gives an estimation of inorganic contents.
What is acid insoluble?
The Acid Insoluble Ash (AIA) content is the proportion of a sample that is not hydrolysed by 72% sulphuric acid and is not subsequently volatilised upon the incineration of this Acid Insoluble Residue.
What is total ash value?
The total ash is the residue remaining after incineration. The acid insoluble ash is the part of the total ash which is insoluble in diluted hydrochloric acid. … Ash values are helpful in determining the quality and purity of the crude drugs in powder form.
What is acid insoluble ash?
Acid-insoluble ash consists primarily of silica and silicates. This material, when present in the finished paper or paperboard, can have an abrasive effect on punches, knives, slitters and dies which come into contact with paper during finishing operations.